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The article is devoted to the adaptation of the controller parameters during its operation as a part of a control loop. The possibility to identify the parameters of the controlled plant model in the closed control loop has been proved by a computer simulation. The described active identification method is based on the response processing of the closed loop control system to standard actions. The developed algorithm has been applied to determine the model parameters of the flaming fluorination reactor used for the production of uranium hexafluoride. Designed identification method improves the quality of the product and the efficiency of the entire production.