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The liquid-phase oxidative destruction of 30% solution of tributyl рhosphate in kerosene has been carried out under the action of oxidants generated by the electrical current which has been passed through 40% aqueous solutions of the sulfuric acid under atmospheric pressure and at temperature of 50 °C. Tributyl phosphate and its solvent have been partly destroyed due to the electrochemical processes on the lead electrodes, however, a large part of components has been subjected to deep oxidation in the volume of electrolyte. As a result of oxidation, the following final products have been formed: phosphoric acid, mono- and dicarboxylic acids, carbon dioxide and water.