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The results of the experimental investigations on sulphur hexafluoride decomposition in the oxigen mixture under the action of a pulse electron beam have been represented. The investigations were performed on the specialized TEA-500 pulse electron accelerator. The parameters of the electron beam are as follows: the electron energy is 450-500 keV, half-amplitude pulse duration is 60 ns, the pulse energy is up to 200 J, the beam diameter is 5 cm. The electron beam was injected to the closed reactor through an anode foil (Al, 140 ?m) from the end. The reactor was a stainless steel cylinder with the inner diameter of 20 cm and the volume of 6 l. The impact of the pulse electron beam on sulphur hexafluoride and the mixture of sulphur hexafluoride and oxygen has been studied. We have obtained the data indicating the chemical reaction whose product is sulphur that X-ray fluorescent analysis confirms.