Interaction of lithium-titanium ceramics with air during sintering / S. A. Gyngazov (Ghyngazov), E. N. Lysenko, M. S. Petyukevich, Т. S. Frangulyan (Franguljyan)

Уровень набора: Russian Physics JournalАльтернативный автор-лицо: Gyngazov (Ghyngazov), S. A., specialist in the field of electronics, Leading researcher of Tomsk Polytechnic University, Doctor of technical sciences, 1958-, Sergey Anatolievich;Lysenko, E. N., Specialist in the field of electrical engineering, Head of the laboratory of Tomsk Polytechnic University, Candidate of physical and mathematical sciences, 1972-, Elena Nikolaevna;Petyukevich, M. S., Specialist in the field of material science, Engineer of Tomsk Polytechnic University, 1982-, Mariya Stanislavovna;Frangulyan (Franguljyan), Т. S., specialist in the field of electronics, dielectrics and semiconductors, leading researcher of Tomsk Polytechnic University, candidate of physical and mathematical Sciences, 1940-, Tamara SemenovnaЯзык: английский.Резюме или реферат: Interaction of lithium-titanium polycrystalline ferrites with ambient air during their sintering is investigated using the methods of electroconductivity and thermal gravimetry within the temperature interval T = 600-1300 K. It is found out that the temperatures exceeding T = 1100 K correspond to effective course of reducing reactions in this material, which results in the formation of an oxygen-deficient ceramic structure in the stage of isothermal tempering (T = 1280 K). It is shown that in the final cooling stage the process of exchange of the ferrite ceramics with the ambient atmosphere exhibits a pronounced oxidative character. The role of these redox processes in the formation of the oxygen non-stoichiometry of the sintered specimen and the depth of its distribution are analyzed..Примечания о наличии в документе библиографии/указателя: [References: p. 139 (7 tit.)].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | lithium-titanium | sintering | ceramics Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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[References: p. 139 (7 tit.)]

Interaction of lithium-titanium polycrystalline ferrites with ambient air during their sintering is investigated using the methods of electroconductivity and thermal gravimetry within the temperature interval T = 600-1300 K. It is found out that the temperatures exceeding T = 1100 K correspond to effective course of reducing reactions in this material, which results in the formation of an oxygen-deficient ceramic structure in the stage of isothermal tempering (T = 1280 K). It is shown that in the final cooling stage the process of exchange of the ferrite ceramics with the ambient atmosphere exhibits a pronounced oxidative character. The role of these redox processes in the formation of the oxygen non-stoichiometry of the sintered specimen and the depth of its distribution are analyzed.

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