Synthesis of Al[2]O[3]-ZrO[2] powders from differently concentrated suspensions with a spray drying technique / G. V. Lyamina [et al.]

Уровень набора: (RuTPU)RU\TPU\network\4816, AIP Conference ProceedingsАльтернативный автор-лицо: Lyamina, G. V., chemist, Associate Professor of Tomsk Polytechnic University, Candidate of chemical sciences, 1974-, Galina Vladimirovna;Ilela, A. E., specialist in the field of material science, Assistant of the Department of Tomsk Polytechnic University, 1982-, Alfa Edison;Khasanov, O. L., Russian physicist, materials scientist, Doctor of Engineering, professor, Director of TPU Nano-Centre and Head of the Department "Nanomaterials and Nanotechnologies" of TPU, 1958-, Oleg Leonidovich;Petyukevich, M. S., Specialist in the field of material science, Engineer of Tomsk Polytechnic University, 1982-, Mariya Stanislavovna;Vaytulevich (Vaitulevich), E. A., chemist, senior lecturer of Tomsk Polytechnic University, candidate of chemical sciences, 1967-, Elena AnatolievnaКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет (ТПУ), Институт физики высоких технологий (ИФВТ), Кафедра общей химии и химической технологии (ОХХТ);Национальный исследовательский Томский политехнический университет (ТПУ), Институт физики высоких технологий (ИФВТ), Кафедра наноматериалов и нанотехнологий (НМНТ)Язык: английский.Серия: Synthesis and physicochemical characteristics of materialsРезюме или реферат: The composite powders of aluminium and zirconium oxides containing 10, 50 and 90 mol % Al{3+} without a stabilizer have been obtained from suspensions using a spray drying method. The powders obtained at equal mole ratios of zirconium and aluminum in the original solution (0.5:0.5 mol/l) have the largest contents of cubic and tetragonal phases of ZrO[2], strictly uniform distribution of phases and the largest value of the specific surface area. The particles with two different morphologies have been obtained: crystalline particles of oxides uniformly distributed in a particle and particles in membrane consisting of zirconium oxide or mixed oxides. It has been experimentally shown that zirconium oxide stabilizes the amorphous phase of aluminum oxide, and aluminum oxide increases the temperature of crystallization of zirconium oxide..Примечания о наличии в документе библиографии/указателя: [References: 11 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | синтез | порошки | суспензии | сушка распылением | композиционные порошки | оксид циркония | кристаллизация Ресурсы он-лайн:Щелкните здесь для доступа в онлайн | Щелкните здесь для доступа в онлайн
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[References: 11 tit.]

The composite powders of aluminium and zirconium oxides containing 10, 50 and 90 mol % Al{3+} without a stabilizer have been obtained from suspensions using a spray drying method. The powders obtained at equal mole ratios of zirconium and aluminum in the original solution (0.5:0.5 mol/l) have the largest contents of cubic and tetragonal phases of ZrO[2], strictly uniform distribution of phases and the largest value of the specific surface area. The particles with two different morphologies have been obtained: crystalline particles of oxides uniformly distributed in a particle and particles in membrane consisting of zirconium oxide or mixed oxides. It has been experimentally shown that zirconium oxide stabilizes the amorphous phase of aluminum oxide, and aluminum oxide increases the temperature of crystallization of zirconium oxide.

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