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[References: 22 tit.]

The possibility of ion exchange technique with of IC-H Hypersep cartridge (Metrohm, Switzerland), sulfonated cation-exchange resins KU-2-8 (Russia) and Purolite C100 (UK) has been shown for ion separation of Mn (II), Fe(III), Cu(II) and Ni(II) ions from arsenite and arsenate ions. The conditions for ion-exchange removal of interfering cations in water when determining different arsenic(III, V) by stripping voltammetry have been optimized. The KU-2-8 cation-exchange resin based cartridge was found to be appropriate for use in the proposed sample preparation for water. The developed technique of analysis has been applied for the separated determination of inorganic arsenic forms in waters of different origin by anodic stripping voltammetry. The correctness of experimental results has been confirmed by the standard addition method.