TiO2 nanoparticle detection by means of laser beam scattering in a hollow cathode plasma jet / R. V. Perekrestov [et al.]

Уровень набора: Journal of Physics D: Applied Physics = 1950-Альтернативный автор-лицо: Perekrestov, R. V., Roman Vyacheslavovich;Kudrna, P.;Tychi, M., Milan;Khalakhan, I., Ivan;Myshkin (Mishkin), V. F., Physicist, Professor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences, 1962-, Vyacheslav FedorovichКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет (ТПУ), Физико-технический институт (ФТИ), Кафедра технической физики (№ 23) (ТФ)Язык: английский.Резюме или реферат: The distribution of TiO2 nanoparticles in a plasma plume of a hollow cathode plasma jet is being studied in this work. The method is based on the detection of light from a laser beam scattered on nanoparticles by three detectors: a photodiode, an optical spectrometer and a digital photo camera. The Rayleigh–Mie theory was used as a basis for the description of the results. Two lasers with wavelengths of 446 and 661?nm were used as light sources. 2D maps of the scattered light intensity were assembled from photo camera pictures at different discharge parameters. Dependencies of the signal intensity on the O2 flow rate and wavelength are discussed. Direct measurements of particle size on the substrate were carried out by means of a scanning electron microscope in order to verify the agreement of results with the theory. Aside from nanoparticles we detected TiO2 columnar structures in the deposited samples. Crystalline structure of the samples was investigated using x-ray diffraction analysis..Примечания о наличии в документе библиографии/указателя: [References: 37 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | наночастицы | оксид титана | лазерные лучи | плазменные струи Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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[References: 37 tit.]

The distribution of TiO2 nanoparticles in a plasma plume of a hollow cathode plasma jet is being studied in this work. The method is based on the detection of light from a laser beam scattered on nanoparticles by three detectors: a photodiode, an optical spectrometer and a digital photo camera. The Rayleigh–Mie theory was used as a basis for the description of the results. Two lasers with wavelengths of 446 and 661?nm were used as light sources. 2D maps of the scattered light intensity were assembled from photo camera pictures at different discharge parameters. Dependencies of the signal intensity on the O2 flow rate and wavelength are discussed. Direct measurements of particle size on the substrate were carried out by means of a scanning electron microscope in order to verify the agreement of results with the theory. Aside from nanoparticles we detected TiO2 columnar structures in the deposited samples. Crystalline structure of the samples was investigated using x-ray diffraction analysis.

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