Thermal effects of carbonated hydroxyapatite modified by glycine and albumin / S. A. Gerk, O. A. Golovanova, M. V. Kuimova

Уровень набора: (RuTPU)RU\TPU\network\2008, IOP Conference Series: Materials Science and EngineeringОсновной Автор-лицо: Gerk, S. A.Альтернативный автор-лицо: Golovanova, O. A.;Kuimova, M. V., linguist, Head of the Department of Tomsk Polytechnic University, Candidate of pedagogical sciences, 1976-, Marina ValerievnaКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет (ТПУ), Физико-технический институт (ФТИ), Кафедра иностранных языков физико-технического института (ИЯФТ)Язык: английский.Серия: Physical and chemical phenomena in inorganic materials in radiation, electrical and thermal fieldsРезюме или реферат: In this work calcium phosphate powders were obtained by precipitation method from simulated solutions of synovial fluid containing glycine and albumin. X-ray diffraction and IR spectroscopy determined that all samples are single-phase and are presented by carbonate containing hydroxyapatite (CHA). The thermograms of solid phases of CHA were obtained and analyzed; five stages of transformation in the temperature range of 25-1000°C were marked. It is shown that in this temperature range dehydration, decarboxylation and thermal degradation of amino acid and protein connected to the surface of solid phase occur. The tendency of temperature lowering of the decomposition of powders synthesized from a medium containing organic substances was determined. Results demonstrate a direct dependence between the concentration of the amino acid in a model solution and its content in the solid phase..Примечания о наличии в документе библиографии/указателя: [References: 27 tit.].Тематика: электронный ресурс | труды учёных ТПУ | термический эффект | гидроксиапатиты | глицин | фосфат кальция | осаждение | рентгеновские лучи | ИК-спектроскопия | порошки | аминокислоты | модельные растворы | твердые фазы Ресурсы он-лайн:Щелкните здесь для доступа в онлайн | Щелкните здесь для доступа в онлайн
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[References: 27 tit.]

In this work calcium phosphate powders were obtained by precipitation method from simulated solutions of synovial fluid containing glycine and albumin. X-ray diffraction and IR spectroscopy determined that all samples are single-phase and are presented by carbonate containing hydroxyapatite (CHA). The thermograms of solid phases of CHA were obtained and analyzed; five stages of transformation in the temperature range of 25-1000°C were marked. It is shown that in this temperature range dehydration, decarboxylation and thermal degradation of amino acid and protein connected to the surface of solid phase occur. The tendency of temperature lowering of the decomposition of powders synthesized from a medium containing organic substances was determined. Results demonstrate a direct dependence between the concentration of the amino acid in a model solution and its content in the solid phase.

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