Calcium Phosphate Targets for RF Magnetron Sputtering of Biocoatings / A. A. Bolat-ool, K. A. Prosolov, M. A. Khimich [et al.]

Уровень набора: (RuTPU)RU\TPU\network\4816, AIP Conference ProceedingsАльтернативный автор-лицо: Bolat-ool, A. A., Anna;Prosolov, K. A., Physicist, Junior research fellow of Tomsk Polytechnic University, 1991-, Konstantin Alexandrovich;Khimich, M. A., Margarita;Chebodaeva, V. V., physicist, technician of Tomsk Polytechnic University, 1991-, Valentina Vadimovna;Uvarkin, P. V., Pavel;Tolmachev, A. I., Alexey;Belyavskaya, O. A., Olga;Sharkeev, Yu. P., physicist, Professor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences, 1950-, Yury PetrovichКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет, Исследовательская школа физики высокоэнергетических процессов, (2017- )Язык: английский.Резюме или реферат: The surface modification of implants became of vital importance for medical field. One of the promising techniques allowing to deposit biocoatings with tailored properties including antibacterial activity is an RF magnetron sputtering. The material of the sputtering target that is going to be deposited on the surface of an implant can be made from various calcium phosphates. Here we present the results of Zn- and Cu-substituted hydroxyapatites and pure hydroxyapatite materials synthesised by mechanochemical method that were sintered in the form of targets for subsequent RF magnetron sputtering. With a set of analytical methods and physico-mechanical testing including X-ray diffraction analysis, energy-dispersive spectroscopy, microhardness measurements and the texture analysis it was shown that the approaches and regimes described in the paper allowed us to produce targets with desired phase composition and good mechanical properties. We estimated the influence of specific surface area of initial calcium phosphate powder with various hydroxyapatite compositions on sintered targets' microhardness. It is concluded that the use of powders with specific surface area in the range of 40-60 m{2} /g is beneficial for formation and sintering of targets with high physicomechanical parameters..Примечания о наличии в документе библиографии/указателя: [References: 11 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | мишени | фосфаты кальция | магнетронное распыление | биопокрытия | имплантаты | гидроксиапатиты | микротвердость Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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[References: 11 tit.]

The surface modification of implants became of vital importance for medical field. One of the promising techniques allowing to deposit biocoatings with tailored properties including antibacterial activity is an RF magnetron sputtering. The material of the sputtering target that is going to be deposited on the surface of an implant can be made from various calcium phosphates. Here we present the results of Zn- and Cu-substituted hydroxyapatites and pure hydroxyapatite materials synthesised by mechanochemical method that were sintered in the form of targets for subsequent RF magnetron sputtering. With a set of analytical methods and physico-mechanical testing including X-ray diffraction analysis, energy-dispersive spectroscopy, microhardness measurements and the texture analysis it was shown that the approaches and regimes described in the paper allowed us to produce targets with desired phase composition and good mechanical properties. We estimated the influence of specific surface area of initial calcium phosphate powder with various hydroxyapatite compositions on sintered targets' microhardness. It is concluded that the use of powders with specific surface area in the range of 40-60 m{2} /g is beneficial for formation and sintering of targets with high physicomechanical parameters.

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