Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage / E. V. Podrezova, M. S. Larkina, M. S. Yusubov [et al.]
Уровень набора: Pharmaceutical Chemistry JournalЯзык: английский.Страна: .Резюме или реферат: A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision..Примечания о наличии в документе библиографии/указателя: [References: 7 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | cyclohexanone | quantitative determination | oxidative cleavage | validation | gas chromatography | internal standard | циклогексанон | количественное определение | окислительное расщепление | газовая хроматография | внутренние стандарты Ресурсы он-лайн:Щелкните здесь для доступа в онлайнНет реальных экземпляров для этой записи
Title screen
[References: 7 tit.]
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
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