Soft X-ray diffraction patterns measured by a LiF detector with sub-micrometre resolution and an ultimate dynamic range / S. Makarov , S. Pikuz, S. Ryazantsev [et al.]

Уровень набора: Journal of Synchrotron RadiationАльтернативный автор-лицо: Makarov, S., Sergey;Pikuz, S., Sergey;Ryazantsev, S., Sergey;Pikuz, T., Tatiana;Buzmakov, A., Alexey;Rose, M., Max;Lazarev, S. V., physicist, engineer at Tomsk Polytechnic University, 1984-, Sergey Vladimirovich;Senkbeil, T., Tobias;Von Gundlach, A., Andreas;Stuhr, S., Susan;Rumancev, C., Christoph;Dzhigaev, D., Dmitry;Skopintsev, P., Petr;Zaluzhnyy, I., Ivan;Viefhaus, J., JensКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет, Институт неразрушающего контроля, Международная научно-образовательная лаборатория неразрушающего контроляЯзык: английский.Страна: .Резюме или реферат: The unique diagnostic possibilities of X-ray diffraction, small X-ray scattering and phase-contrast imaging techniques applied with high-intensity coherent X-ray synchrotron and X-ray free-electron laser radiation can only be fully realized if a sufficient dynamic range and/or spatial resolution of the detector is available. In this work, it is demonstrated that the use of lithium fluoride (LiF) as a photoluminescence (PL) imaging detector allows measuring of an X-ray diffraction image with a dynamic range of ~10⁷ within the sub-micrometre spatial resolution. At the PETRA III facility, the diffraction pattern created behind a circular aperture with a diameter of 5 µm irradiated by a beam with a photon energy of 500 eV was recorded on a LiF crystal. In the diffraction pattern, the accumulated dose was varied from 1.7 ˣ 10⁵ J cm⁻³ in the central maximum to 2 ˣ 10⁻² J cm⁻³ in the 16th maximum of diffraction fringes. The period of the last fringe was measured with 0.8 µm width. The PL response of the LiF crystal being used as a detector on the irradiation dose of 500 eV photons was evaluated. For the particular model of laser-scanning confocal microscope Carl Zeiss LSM700, used for the readout of the PL signal, the calibration dependencies on the intensity of photopumping (excitation) radiation (λ = 488 nm) and the gain have been obtained..Тематика: электронный ресурс | труды учёных ТПУ | diffraction patterns | LiF detectors | color centers | дифракционные картины | центры окраски | детекторы LiF | рентгеновское излучение | лазеры | X-Ray | lasers Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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The unique diagnostic possibilities of X-ray diffraction, small X-ray scattering and phase-contrast imaging techniques applied with high-intensity coherent X-ray synchrotron and X-ray free-electron laser radiation can only be fully realized if a sufficient dynamic range and/or spatial resolution of the detector is available. In this work, it is demonstrated that the use of lithium fluoride (LiF) as a photoluminescence (PL) imaging detector allows measuring of an X-ray diffraction image with a dynamic range of ~10⁷ within the sub-micrometre spatial resolution. At the PETRA III facility, the diffraction pattern created behind a circular aperture with a diameter of 5 µm irradiated by a beam with a photon energy of 500 eV was recorded on a LiF crystal. In the diffraction pattern, the accumulated dose was varied from 1.7 ˣ 10⁵ J cm⁻³ in the central maximum to 2 ˣ 10⁻² J cm⁻³ in the 16th maximum of diffraction fringes. The period of the last fringe was measured with 0.8 µm width. The PL response of the LiF crystal being used as a detector on the irradiation dose of 500 eV photons was evaluated. For the particular model of laser-scanning confocal microscope Carl Zeiss LSM700, used for the readout of the PL signal, the calibration dependencies on the intensity of photopumping (excitation) radiation (λ = 488 nm) and the gain have been obtained.

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