Synthesis and characterization of zinc oxide nanopowder / M. V. Zhuravlev, R. V. Sazonov, G. E. Kholodnaya [et al.]
Уровень набора: Inorganic and Nano-Metal ChemistryЯзык: английский.Страна: .Резюме или реферат: Several batches of zinc oxide (ZnO) nanopowders were obtained using the electrospark method. The samples differed in starting reagents. The electrospark method for producing ZnO nanoparticles is based on using the energy of an electric spark discharge generated between the electrode and the target. The morphology and phase composition of the synthesized samples were studied. The average particle size ranged from 10 to 25?nm. Particle morphology was diverse and represented mainly by flake nanoparticles. We recorded peaks characteristic of zinc and intensive peaks characteristic of ZnO on the X-ray pattern. The calculated sizes corresponded to coherent scattering for the crystalline phases of ZnO. The band gap was calculated for the synthesis of ZnO nanopowders. A slight narrowing of the band gap indicated the predominant crystalline phase in ZnO nanoparticles and an insignificant effect of the surface states of growth defects..Примечания о наличии в документе библиографии/указателя: [References: 56 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | electrospark method | zinc oxide | flake nanoparticles | электроискровые методы | оксид цинка | наночастицы Ресурсы он-лайн:Щелкните здесь для доступа в онлайнTitle screen
[References: 56 tit.]
Several batches of zinc oxide (ZnO) nanopowders were obtained using the electrospark method. The samples differed in starting reagents. The electrospark method for producing ZnO nanoparticles is based on using the energy of an electric spark discharge generated between the electrode and the target. The morphology and phase composition of the synthesized samples were studied. The average particle size ranged from 10 to 25?nm. Particle morphology was diverse and represented mainly by flake nanoparticles. We recorded peaks characteristic of zinc and intensive peaks characteristic of ZnO on the X-ray pattern. The calculated sizes corresponded to coherent scattering for the crystalline phases of ZnO. The band gap was calculated for the synthesis of ZnO nanopowders. A slight narrowing of the band gap indicated the predominant crystalline phase in ZnO nanoparticles and an insignificant effect of the surface states of growth defects.
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