Microstructure and electromagnetic properties of LiFe5O8 ferrite ceramics prepared from wet- and dry-milled powders / E. N. Lysenko, V. A. Vlasov, A. V. Malyshev [et al.]

Уровень набора: Ceramics InternationalАльтернативный автор-лицо: Lysenko, E. N., Specialist in the field of electrical engineering, Head of the laboratory of Tomsk Polytechnic University, Candidate of physical and mathematical sciences, 1972-, Elena Nikolaevna;Vlasov, V. A., Physicist, Senior researcher of Tomsk Polytechnic University, Candidate of physical and mathematical sciences, 1975-, Vitaliy Anatolievich;Malyshev, A. V., Specialist in the field of electrical engineering, Senior researcher at Tomsk Polytechnic University, Candidate of Physics and Mathematics (PhD Phys.-Math.), 1978-, Andrei Vladimirovich;Sheveleva, E. A., specialist in the field of electrical engineering, Associate Professor of Tomsk Polytechnic University, Candidate of technical sciences, 1975-, Elena Aleksandrovna;Surzhikov, A. P., physicist, Professor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc), 1951-, Anatoly PetrovichКоллективный автор (вторичный): Национальный исследовательский Томский политехнический университет, Институт неразрушающего контроля, Проблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводниковЯзык: английский.Резюме или реферат: The effect of dry and wet ball milling of LiFe5O8 ferrite powder on the microstructure and electromagnetic properties of ferrite ceramics was studied using XRD analysis, scanning electron microscopy, dilatometry, thermogravimetry, calorimetry, and measurement of specific magnetization and electrical resistance. The sintering temperature was 1050 °C; the sintering time was 2 h. It was found that ferrite fabricated from dry-milled powder exhibits an ordered [alpha]-LiFe5O8 phase with bulk density of 91%. Its saturation magnetization and Curie temperature are 55 emu/g and 628°С, respectively. Specific electrical resistance is 4•106 [omega] cm. Wet milling in isopropyl alcohol causes formation of a disordered [beta]-LiFe5O8 phase. Ceramics produced by this method shows higher bulk density (97%) and low porosity, and an order of magnitude lower resistivity. Its saturation magnetization and Curie temperature are 51 emu/g and 607°С, respectively..Примечания о наличии в документе библиографии/указателя: [References: 54 tit.].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | sintering | electrical properties | magnetic properties | ferrites | спекание | электрические свойства | магнитные свойства | ферриты Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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[References: 54 tit.]

The effect of dry and wet ball milling of LiFe5O8 ferrite powder on the microstructure and electromagnetic properties of ferrite ceramics was studied using XRD analysis, scanning electron microscopy, dilatometry, thermogravimetry, calorimetry, and measurement of specific magnetization and electrical resistance. The sintering temperature was 1050 °C; the sintering time was 2 h. It was found that ferrite fabricated from dry-milled powder exhibits an ordered [alpha]-LiFe5O8 phase with bulk density of 91%. Its saturation magnetization and Curie temperature are 55 emu/g and 628°С, respectively. Specific electrical resistance is 4•106 [omega] cm. Wet milling in isopropyl alcohol causes formation of a disordered [beta]-LiFe5O8 phase. Ceramics produced by this method shows higher bulk density (97%) and low porosity, and an order of magnitude lower resistivity. Its saturation magnetization and Curie temperature are 51 emu/g and 607°С, respectively.

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