Influence of mechanical activation of initial reagents on synthesis of lithium ferrite / A. P. Surzhikov [et al.]

Уровень набора: Russian Physics Journal, Scientific JournalАльтернативный автор-лицо: Surzhikov, A. P., physicist, Professor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc), 1951-, Anatoly Petrovich;Lysenko, E. N., Specialist in the field of electrical engineering, Head of the laboratory of Tomsk Polytechnic University, Candidate of physical and mathematical sciences, 1972-, Elena Nikolaevna;Malyshev, A. V., Specialist in the field of electrical engineering, Senior researcher at Tomsk Polytechnic University, Candidate of Physics and Mathematics (PhD Phys.-Math.), 1978-, Andrei Vladimirovich;Pritulov, A. M.;Kazakovskaya, O. G.Коллективный автор (вторичный): Национальный исследовательский Томский политехнический университет (ТПУ), Институт неразрушающего контроля (ИНК), Проблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников (ПНИЛ ЭДиП)Язык: английский.Резюме или реферат: The influence of mechanical activation of the Li2CO3–Fe2O3 initial reagents on ferrite phase formation in lithium ferrite LiFe5O8 is investigated. Methods of x-ray powder diffraction (XRD) and thermomagnetometry with differential scanning calorimetry (TG(M)/DSC) are used to compare the efficiency of nonisothermal synthesis at identical temperatures and burning times of the initial and mechanically activated reagent mixtures. It is demonstrated that preliminary mechanical activation of the initial Li2CO3–Fe2O3 reagent mixture considerably increases the reactivity of the solid phase system, thereby allowing the temperature of the thermal synthesis of lithium ferrite LiFe5O8 to be decreased significantly..Примечания о наличии в документе библиографии/указателя: [References: p. 677 (15 tit.)].Аудитория: .Тематика: электронный ресурс | труды учёных ТПУ | lithium ferrite | LiFe5O8 | solid phase synthesis | mechanical activation | TG(M)/DSC | XRP Ресурсы он-лайн:Щелкните здесь для доступа в онлайн
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[References: p. 677 (15 tit.)]

The influence of mechanical activation of the Li2CO3–Fe2O3 initial reagents on ferrite phase formation in lithium ferrite LiFe5O8 is investigated. Methods of x-ray powder diffraction (XRD) and thermomagnetometry with differential scanning calorimetry (TG(M)/DSC) are used to compare the efficiency of nonisothermal synthesis at identical temperatures and burning times of the initial and mechanically activated reagent mixtures. It is demonstrated that preliminary mechanical activation of the initial Li2CO3–Fe2O3 reagent mixture considerably increases the reactivity of the solid phase system, thereby allowing the temperature of the thermal synthesis of lithium ferrite LiFe5O8 to be decreased significantly.

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