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100 _a20150325a2012 k y0engy50 ba
101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aInfluence of mechanical activation of initial reagents on synthesis of lithium ferrite
_fA. P. Surzhikov [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: p. 677 (15 tit.)]
330 _aThe influence of mechanical activation of the Li2CO3–Fe2O3 initial reagents on ferrite phase formation in lithium ferrite LiFe5O8 is investigated. Methods of x-ray powder diffraction (XRD) and thermomagnetometry with differential scanning calorimetry (TG(M)/DSC) are used to compare the efficiency of nonisothermal synthesis at identical temperatures and burning times of the initial and mechanically activated reagent mixtures. It is demonstrated that preliminary mechanical activation of the initial Li2CO3–Fe2O3 reagent mixture considerably increases the reactivity of the solid phase system, thereby allowing the temperature of the thermal synthesis of lithium ferrite LiFe5O8 to be decreased significantly.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tRussian Physics Journal
_oScientific Journal
463 _tVol. 55, iss. 6
_v[P. 672-677]
_d2012
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _alithium ferrite
610 1 _aLiFe5O8
610 1 _asolid phase synthesis
610 1 _amechanical activation
610 1 _aTG(M)/DSC
610 1 _aXRP
701 1 _aSurzhikov
_bA. P.
_cphysicist
_cProfessor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc)
_f1951-
_gAnatoly Petrovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30237
701 1 _aLysenko
_bE. N.
_cSpecialist in the field of electrical engineering
_cHead of the laboratory of Tomsk Polytechnic University, Candidate of physical and mathematical sciences
_f1972-
_gElena Nikolaevna
_2stltpush
_3(RuTPU)RU\TPU\pers\32050
701 1 _aMalyshev
_bA. V.
_cSpecialist in the field of electrical engineering
_cSenior researcher at Tomsk Polytechnic University, Candidate of Physics and Mathematics (PhD Phys.-Math.)
_f1978-
_gAndrei Vladimirovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30965
701 1 _aPritulov
_bA. M.
701 1 _aKazakovskaya
_bO. G.
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bИнститут неразрушающего контроля (ИНК)
_bПроблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников (ПНИЛ ЭДиП)
_h194
_2stltpush
_3(RuTPU)RU\TPU\col\19033
801 2 _aRU
_b63413507
_c20160321
_gRCR
856 4 _uhttp://dx.doi.org/10.1007/s11182-012-9865-7
942 _cCF