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100 _a20150513a2015 k y0engy50 ba
101 0 _aeng
102 _aUS
105 _ay z 100zy
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aKinetic Analysis of Lithium-Zinc Ferrite Synthesis by Thermogravimetric Method
_fE. V. Nikolaev, A. P. Surzhikov, E. N. Lysenko
203 _aText
_celectronic
225 1 _aStructure Materials, Mechanics and Dynamics of Materials
300 _aTitle screen
330 _aThe kinetic of lithium-zinc ferrite synthesis reaction up to temperatures 800°С was studied in air using non-isothermal thermogravimetric analysis. Mathematical treatment of thermogravimetric curves was carried out using Netzsch Thermokinetics software where the kinetic model with minimal adjustable parameters quantitatively describe the synthesis reaction of lithium-zinc ferrite was chosen. It was shown that the experimental TG curves clearly suggest a multi-step process for the ferrite synthesis and therefore a model-fitting kinetic analysis based on multivariate non-linear regressions was conducted. The complex reaction can be best described with a three-step reaction scheme consisting of parallel reaction steps. It is established that the best results were obtained with the using at the first stage the diffusion model of Yander, on the second and third stage were used the reactions of n-order. Kinetic parameters of lithium-zinc ferrite synthesis reaction were found.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 0 _0(RuTPU)RU\TPU\network\4598
_tAdvanced Materials Research
_oScientific Journal
463 0 _0(RuTPU)RU\TPU\network\4656
_tVol. 1085 : Prospects of Fundamental Sciences Development (PFSD-2014)
_oThe XIth International Conference, April 22-25, 2014, Tomsk, Russia
_o[proceedings]
_v[P. 255-259]
_d2015
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aкинетические модели
610 1 _aкинетические параметры
610 1 _aлитий-цинковые ферриты
700 1 _aNikolaev
_bE. V.
_cspecialist in the field of electrical engineering
_cengineer of Tomsk Polytechnic University
_f1989-
_gEvgeny Vladimirovich
_2stltpush
_3(RuTPU)RU\TPU\pers\34529
701 1 _aSurzhikov
_bA. P.
_cphysicist
_cProfessor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc)
_f1951-
_gAnatoly Petrovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30237
701 1 _aLysenko
_bE. N.
_cSpecialist in the field of electrical engineering
_cHead of the laboratory of Tomsk Polytechnic University, Candidate of physical and mathematical sciences
_f1972-
_gElena Nikolaevna
_2stltpush
_3(RuTPU)RU\TPU\pers\32050
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bИнститут неразрушающего контроля (ИНК)
_bПроблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников (ПНИЛ ЭДиП)
_h194
_2stltpush
_3(RuTPU)RU\TPU\col\19033
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bИнститут неразрушающего контроля (ИНК)
_bКафедра физических методов и приборов контроля качества (ФМПК)
_h68
_2stltpush
_3(RuTPU)RU\TPU\col\18709
801 2 _aRU
_b63413507
_c20161229
_gRCR
856 4 _uhttp://dx.doi.org/10.4028/www.scientific.net/AMR.1085.255
942 _cCF