| 000 | 03874nlm1a2200505 4500 | ||
|---|---|---|---|
| 001 | 647440 | ||
| 005 | 20231030040801.0 | ||
| 035 | _a(RuTPU)RU\TPU\network\12580 | ||
| 035 | _aRU\TPU\network\7878 | ||
| 090 | _a647440 | ||
| 100 | _a20160411a2013 k y0engy50 ba | ||
| 101 | 0 | _aeng | |
| 135 | _adrcn ---uucaa | ||
| 181 | 0 | _ai | |
| 182 | 0 | _ab | |
| 200 | 1 |
_aThe structure of an rf-magnetron sputter-deposited silicate-containinghydroxyapatite-based coating investigated by high-resolution techniques _fM. A. Surmeneva [et al.] |
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| 203 |
_aText _celectronic |
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| 300 | _aTitle screen | ||
| 320 | _a[References: p. 46 (44 tit.)] | ||
| 330 | _aA biocompatible nanostructured silicate-containing hydroxyapatite-based (Si-HA) thin coating was deposited by radio-frequency (RF) magnetron sputtering on silicon and titanium substrates. The morphology of the Si-HA coating was pore-free, dense and followed the topography of the underlying substrates. Energy-dispersive X-ray spectroscopy (EDX) gave molar Ca/P and Ca/(P + Si) ratios of 1.78 and 1.45, respectively. According to XRD-analysis, the coating was nanocrystalline with a crystallite size in the range of 10-50 nm. The ultrastructure of the coating was analyzed by high-resolution transmission electron spectroscopy (HRTEM) combined with fast Fourier transform (FFT) analysis. The average crystallite size calculated by the Rietveld method was in good agreement with the HRTEM results. Moreover, HRTEM-observations indicated the presence of atomic layer misorientations originating from imperfections between the nanocrystals in the coating. The average coating nanohardness (11.6 ± 1.7 GPa) was significantly higher than that of the uncoated Ti substrate (4.0 ± 0.3 GPa), whereas no significant difference between the Young's modulus of the coating (125 ± 20 GPa) and the substrate (115 ± 10 GPa) was found. Immersion of the coated substrates in simulated body fluid (SBF) led to the deposition of an apatite layer. | ||
| 333 | _aРежим доступа: по договору с организацией-держателем ресурса | ||
| 461 | _tSurface and Coatings Technology | ||
| 463 |
_tVol. 218 _v[P. 39-46] _d2013 |
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| 610 | 1 | _aэлектронный ресурс | |
| 610 | 1 | _aтруды учёных ТПУ | |
| 610 | 1 | _acalcium phosphate | |
| 610 | 1 | _acoatings | |
| 610 | 1 | _ananocomposites | |
| 610 | 1 | _aimplants | |
| 610 | 1 | _aфосфат кальция | |
| 610 | 1 | _aпокрытия | |
| 610 | 1 | _aнанокомпозиты | |
| 610 | 1 | _aимплантаты | |
| 701 | 1 |
_aSurmeneva (Ryabtseva) _bM. A. _cspecialist in the field of material science _cengineer-researcher of Tomsk Polytechnic University, Associate Scientist _f1984- _gMaria Alexandrovna _2stltpush _3(RuTPU)RU\TPU\pers\31894 |
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| 701 | 1 |
_aChaikina _bM. V. |
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| 701 | 1 |
_aZaikovskiv _bV. I. |
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| 701 | 1 |
_aPichugin _bV. F. _cProfessor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences _cPhysicist _f1944- _gVladimir Fyodorovich _2stltpush _3(RuTPU)RU\TPU\pers\30933 |
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| 701 | 1 |
_aBuck _bV. |
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| 701 | 1 |
_aPrymak _bO. |
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| 701 | 1 |
_aEpple _bM. |
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| 701 | 1 |
_aSurmenev _bR. A. _cphysicist _cAssociate Professor of Tomsk Polytechnic University, Senior researcher, Candidate of physical and mathematical sciences _f1982- _gRoman Anatolievich _2stltpush _3(RuTPU)RU\TPU\pers\31885 |
|
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет (ТПУ) _bФизико-технический институт (ФТИ) _bКафедра теоретической и экспериментальной физики (ТиЭФ) _bЦентр технологий (ЦТ) _h408 _2stltpush _3(RuTPU)RU\TPU\col\20620 |
| 801 | 2 |
_aRU _b63413507 _c20210512 _gRCR |
|
| 856 | 4 | _uhttp://dx.doi.org/10.1016/j.surfcoat.2012.12.023 | |
| 942 | _cCF | ||