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035 _a(RuTPU)RU\TPU\network\12590
035 _aRU\TPU\network\12586
090 _a647450
100 _a20160411a2008 k y0engy50 ba
101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aThe preparation of calcium phosphate coatings on titanium and nickel-titanium by rf-magnetron-sputtered deposition: Composition, structure and micromechanical properties
_fV. F. Pichugin [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: p. 3919-3920 (66 tit.)]
330 _aThin calcium phosphate coatings with a thickness of 0.09 to 2.7 µm were prepared by radio-frequency magnetron sputtering deposition on NiTi and Ti substrates at a substrate temperature of 500 °C in argon atmosphere. Scanning electron microscopy (SEM) showed that the surface structure is uniform and dense without visible defects (pores and microcracks). Rutherford backscattering spectroscopy (RBS) and energy-dispersive X-ray spectroscopy (EDX) confirmed that the coating contains calcium, phosphorus, and oxygen with a uniform composition. Crystallographically, the coating consists of crystalline hydroxyapatite which is also supported by infrared spectroscopy. The mechanical characteristics of the coating were measured by nanoindentation (Vickers indenter), giving a nanohardness of 10 GPa and a Young's modulus of 110 GPa. The strength of adhesion of the calcium phosphate coating to the metallic substrates depended on the coating's thickness and decreased for a thickness larger than 1.6 µm. No difference was observed between NiTi and Ti substrates.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tSurface and Coatings Technology
463 _tVol. 202, iss. 16
_v[P. 3913-3920]
_d2008
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _acoatings
610 1 _acalcium phosphate
610 1 _arf-magnetron sputtering
610 1 _aфосфат кальция
610 1 _aпокрытия
610 1 _aВЧ-магнетронное распыление
610 1 _aнапыление
610 1 _aподложки
610 1 _aмеханические свойства
610 1 _aтитан
610 1 _aникель
610 1 _aсплавы
610 1 _aфосфаты
610 1 _aкальций
701 1 _aPichugin
_bV. F.
_cProfessor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences
_cPhysicist
_f1944-
_gVladimir Fyodorovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30933
701 1 _aSurmenev
_bR. A.
_cphysicist
_cAssociate Professor of Tomsk Polytechnic University, Senior researcher, Candidate of physical and mathematical sciences
_f1982-
_gRoman Anatolievich
_2stltpush
_3(RuTPU)RU\TPU\pers\31885
701 1 _aShesterikov
_bE. V.
_cphysicist
_cleading engineer of Tomsk Polytechnic University
_f1979-
_gEvgeny Viktorovich
_2stltpush
_3(RuTPU)RU\TPU\pers\35793
701 1 _aRyabtseva
_bM. A.
701 1 _aEshenko
_bE. V.
701 1 _aTverdokhlebov
_bS. I.
_cphysicist
_cAssociate Professor of Tomsk Polytechnic University, Candidate of physical and mathematical science
_f1961-
_gSergei Ivanovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30855
701 1 _aPrymak
_bO.
701 1 _aEpple
_bM.
801 2 _aRU
_b63413507
_c20160411
_gRCR
856 4 _uhttp://dx.doi.org/10.1016/j.surfcoat.2008.01.038
942 _cCF