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100 _a20161229a2016 k y0engy50 ba
101 0 _aeng
102 _aNL
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aPlasma dynamic synthesis and obtaining ultradispersed zinc oxide with single-crystalline particle structure
_fA. A. Sivkov [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: p. 1513 (31 tit.)]
330 _aZinc oxide is well-known semiconductor material having good electrical, optical and catalytic properties. This paper shows the results on synthesis of hexagonal zinc oxide with single-crystalline particle structure using the system based on coaxial magnetoplasma accelerator. The synthesis is implemented during one short cycle (up to 10?3 s) of plasma accelerator work. X-ray diffractometry analysis allow us to confirm that the product consists of only hexagonal zinc oxide with lattice parameters a = b = 3.24970 A, c = 5.20270 A. This result is in a good agreement with EDAX data, which show the presence only Zn and O elements in the final product. SEM, TEM and HRTEM methods are used to investigate the particles morphology. It is found that the product consists of single-crystalline hexagonal particles of zinc oxide and electron diffraction from particles also confirmed the zinc oxide structure. The particle sizes are up to 350 nm but the most of the particles (85%) are less than 150 nm.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tAdvanced Powder Technology
_oScientific Journal
463 _tVol. 27, № 4
_v[P. 1506–1513]
_d2016
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aоксид цинка
610 1 _aнаночастицы
610 1 _aускорители
701 1 _aSivkov
_bA. A.
_cSpecialist in the field of electric power engineering
_cProfessor of Tomsk Polytechnic University, Doctor of technical sciences
_f1951-
_gAleksandr Anatolyevich
_2stltpush
_3(RuTPU)RU\TPU\pers\32273
701 1 _aIvashutenko
_bA. S.
_cspecialist in the field of electrical engineering
_cHead of the Department of the Tomsk Polytechnic University, Candidate of technical sciences
_f1981-
_gAlexander Sergeevich
_2stltpush
_3(RuTPU)RU\TPU\pers\33076
701 1 _aShanenkova
_bYu. L.
_cspecialist in the field of electric power engineering
_claboratory assistant of Tomsk Polytechnic University
_f1991-
_gYuliya Leonidovna
_2stltpush
_3(RuTPU)RU\TPU\pers\34119
701 1 _aShanenkov
_bI. I.
_cspecialist in the field of electric power engineering
_cDetailer of Tomsk Polytechnic University
_f1990-
_gIvan Igorevich
_2stltpush
_3(RuTPU)RU\TPU\pers\32880
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bЭнергетический институт (ЭНИН)
_bКафедра электроснабжения промышленных предприятий (ЭПП)
_h186
_2stltpush
_3(RuTPU)RU\TPU\col\18676
801 2 _aRU
_b63413507
_c20161229
_gRCR
856 4 _uhttp://dx.doi.org/10.1016/j.apt.2016.05.012
942 _cCF