000 03280nla2a2200505 4500
001 653838
005 20231030041234.0
035 _a(RuTPU)RU\TPU\network\19353
035 _aRU\TPU\network\19352
090 _a653838
100 _a20170331a2017 k y0engy50 ba
101 0 _aeng
105 _ay z 100zy
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aThermal stability of brushite with chitosan samples
_fE. S. Chikanova [et al.]
203 _aText
_celectronic
225 1 _aTechnologies and equipment for their implementation
300 _aTitle screen
320 _a[References: 9 tit.]
330 _aIn this paper, the powders of brushite from an aqueous solution of Ca(NO[3])[2]- (NH[4])[2]HPO[4] with different content of chitosan were synthesized. XRD data revealed that all samples are single-phase and are brushite (CaHPO[4]•centerdot2H[2]O). By FT-IR spectroscopy and BET methods, it was found that chitosan adsorbs onto the surface of powders. With increase of the content of the additive, the average size of crystallites increases 4.0 – 4.8 – 11.8 [mu]m, respectively, and the dissolution rate in isotonic solution also decreases. The thermal stability of the composite powders was studied. It was established that the highest destruction of samples occurs in the range 473-673 K by removing of adsorption and crystallization water and partial change of the structure of the mineral and chitosan. At a temperature of 873 K, carbonization of the organic additive occurs.
461 0 _0(RuTPU)RU\TPU\network\2008
_tIOP Conference Series: Materials Science and Engineering
463 0 _0(RuTPU)RU\TPU\network\19289
_tVol. 168 : Radiation-Thermal Effects and Processes in Inorganic Materials (RTEP2016)
_oXII International Conference, 4–12 September 2016, Tomsk, Russian Federation
_o[proceedings]
_v[012066, 6 p.]
_d2017
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aтермическая стабильность
610 1 _aбрушит
610 1 _aводные растворы
610 1 _aИК-Фурье спектроскопия
610 1 _aповерхности
610 1 _aпорошки
610 1 _aдобавки
610 1 _aтермическая стабильность
610 1 _aкомпозиционные порошки
610 1 _aкарбонизация
701 1 _aChikanova
_bE. S.
701 1 _aGolovanova
_bО. А.
701 1 _aMalikova
_bT. V.
701 1 _aKuimova
_bM. V.
_clinguist
_cHead of the Department of Tomsk Polytechnic University, Candidate of pedagogical sciences
_f1976-
_gMarina Valerievna
_2stltpush
_3(RuTPU)RU\TPU\pers\32753
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bФизико-технический институт (ФТИ)
_bКафедра иностранных языков физико-технического института (ИЯФТ)
_h6715
_2stltpush
_3(RuTPU)RU\TPU\col\18736
801 2 _aRU
_b63413507
_c20170404
_gRCR
856 4 _uhttp://dx.doi.org/10.1088/1757-899X/168/1/012066
856 4 _uhttp://earchive.tpu.ru/handle/11683/37765
942 _cCF