000			02247nlm1a2200433 4500
001			654279
005			20231030041254.0
035			_a(RuTPU)RU\TPU\network\19873
035			_aRU\TPU\network\19839
090			_a654279
100			_a20170424a2007 k y0engy50 ba
101	0		_aeng
102			_aUS
135			_adrcn ---uucaa
181		0	_ai
182		0	_ab
200	1		_a4-Iodoantipyrine synthesized by means of solid-state mechanical activation _fE. A . Krasnokutskaya [et al.]
203			_aText _celectronic
300			_aTitle screen
320			_a[References: 11 tit.]
330			_aAntipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-.
333			_aРежим доступа: по договору с организацией-держателем ресурса
461			_tPharmaceutical Chemistry Journal
463			_tVol. 41, iss. 3 _v[P. 154-156] _d2007
610	1		_aэлектронный ресурс
610	1		_aтруды учёных ТПУ
610	1		_aсинтез
610	1		_aактивация
610	1		_aантипирин
610	1		_aиодирование
610	1		_aтетраалкиламмониевые соли
610	1		_aзеленая химия
701		1	_aKrasnokutskaya _bE. A . _corganic chemist _cProfessor of Tomsk Polytechnic University, Doctor of chemical sciences _f1966- _gElena Aleksandrovna _2stltpush _3(RuTPU)RU\TPU\pers\31829
701		1	_aTrusova _bM. E. _corganic chemist _cAssociate professor of Tomsk Polytechnic University, Candidate of chemical sciences _f1982- _gMarina Evgenievna _2stltpush _3(RuTPU)RU\TPU\pers\31823
701		1	_aGibert _bN. S.
701		1	_aFilimonov _bV. D. _cRussian chemist _cProfessor of the TPU _f1945- _gViktor Dmitrievich _2stltpush _3(RuTPU)RU\TPU\pers\26423
801		2	_aRU _b63413507 _c20170424 _gRCR
856	4		_uhttp://dx.doi.org/10.1007/s11094-007-0034-1
942			_cCF