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100 _a20170524a2011 k y0engy50 ba
101 0 _aeng
102 _aUS
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aPotentiometric determination of the total acidity and concentration of citric acid in wines
_fE. A. Zakharova [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: p. 853 (12 tit.)]
330 _aThe method of potentiometric titration with a copper electrode is used for the determination of the total acidity and concentration of citric acid (CA) in identifying the adulteration of wines. The procedure is suitable for the determination of citric acid in wines in the range from 0.1 to 3.5 g/L in the presence of 30-fold amounts of tartaric, acetic, malic, succinic acids and a 10-fold amount of oxalic acid after the separation of organic carboxylic acids on an AV-17-8 anion exchanger. The procedure was developed and certified for the potentiometric determination of the mass fraction of citric acid in table wines and wine materials with an error not exceeding 20%. The criteria (mass fraction of citric acid, the percentage of citric acid in the total acidity, and the shape of the curves of potentiometric titration) were proposed for revealing the adulteration of the acid composition of wines.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tJournal of Analytical Chemistry
463 _tVol. 66, iss. 9
_v[P. 848–853]
_d2011
610 1 _aтруды учёных ТПУ
610 1 _aэлектронный ресурс
610 1 _aкислотность
610 1 _aлимонная кислота
610 1 _aвина
610 1 _aанализ
610 1 _aфальсификация
610 1 _aпотенциометрический анализ
610 1 _aтитрование
610 1 _aэлектроды
701 1 _aZakharova
_bE. A.
_cchemist
_csenior research fellow at the Tomsk Polytechnic University, candidate of chemical Sciences
_f1938-
_gElsa Arminana
_2stltpush
_3(RuTPU)RU\TPU\pers\33332
701 1 _aMoskaleva
_bM. L.
701 1 _aAkeneev
_bYu. A.
_cchemist
_cresearcher of Tomsk Polytechnic University
_f1961-
_gYuriy Anvarovich
_2stltpush
_3(RuTPU)RU\TPU\pers\35924
701 1 _aMoiseeva
_bE. S.
_cchemical engineer
_cMetrology Engineer of the second category of Tomsk Polytechnic University, Candidate of chemical sciences
_f1980-
_gEvgeniya Sergeevna
_2stltpush
_3(RuTPU)RU\TPU\pers\45381
701 1 _aSlepchenko
_bG. B.
_cChemist
_cProfessor of Tomsk Polytechnic University, Doctor of chemical sciences
_f1956-
_gGalina Borisovna
_2stltpush
_3(RuTPU)RU\TPU\pers\33018
701 1 _aPikula
_bN. P.
801 2 _aRU
_b63413507
_c20191127
_gPSBO
856 4 _uhttp://dx.doi.org/10.1134/S1061934811090218
942 _cCF