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090 _a655134
100 _a20170704a2017 k y0engy50 ba
101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aEffect of Hydrogen Exposure on Mechanical and Tribological Behavior of CrxN Coatings Deposited at Different Pressures on IN718
_fA. Obrosov [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: 50 tit.]
330 _aIn the current study, the properties of the CrxN coatings deposited on the Inconel 718 superalloy using direct current reactive magnetron sputtering are investigated. The influence of working pressure on the microstructure, mechanical, and tribological properties of the CrxN coatings before and after high-temperature hydrogen exposure is studied. The cross-sectional scanning electron micrographs indicate the columnar structure of the coatings, which changes from dense and compact columns to large columns with increasing working pressure. The Cr/N ratio increases from 1.4 to 1.9 with increasing working pressure from 300 to 900 mPa, respectively. X-ray diffraction analysis reveals a change from mixed hcp-Cr2N and fcc-CrN structure to approximately stoichiometric Cr2N phase. After gas-phase hydrogenation, the coating deposited at 300 mPa exhibits the lowest hydrogen absorption at 600 °C of all investigated coatings. The results indicate that the dense mixed cubic and hexagonal structure is preferential for hydrogen permeation resistance due to the presence of cubic phase with higher packing density in comparison to the hexagonal structure. After hydrogenation, no changes in phase composition were observed; however, a small amount of hydrogen is accumulated in the coatings. An increase of coating hardness and elastic modulus was observed after hydrogen exposure. Tribological tests reveal that hydrogenation leads to a decrease of the friction coefficient up to 20%-30%. The best value of 0.25 was reached for hydrogen exposed CrxN coating deposited at 300 mPa.
461 _tMaterials
463 _tVol. 10, iss. 5
_v[563, 11 p.]
_d2017
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aгидрирование
610 1 _aтрибология
610 1 _aмеханические свойства
610 1 _aCrxN coatings
610 1 _aPVD
610 1 _ahydrogenation
610 1 _atribology
610 1 _aproperties
610 1 _aGDOES
701 1 _aObrosov
_bA.
_gAleksey
701 1 _aSutygina
_bA. N.
_cPhysicist
_cTechnician of Tomsk Polytechnic University
_f1993-
_gAlina Nikolaevna
_2stltpush
_3(RuTPU)RU\TPU\pers\37677
701 1 _aVolinsky
_bA.
_gAlex
701 1 _aManakhov
_bA.
_gAnton
701 1 _aWeifs
_bS.
_gSabine
701 1 _aKashkarov
_bE. B.
_cPhysicist
_cEngineer of Tomsk Polytechnic University
_f1991-
_gEgor Borisovich
_2stltpush
_3(RuTPU)RU\TPU\pers\34949
712 0 2 _aНациональный исследовательский Томский политехнический университет (ТПУ)
_bФизико-технический институт (ФТИ)
_bКафедра общей физики (ОФ)
_h136
_2stltpush
_3(RuTPU)RU\TPU\col\18734
801 2 _aRU
_b63413507
_c20170704
_gRCR
856 4 _uhttp://dx.doi.org/10.3390/ma10050563
942 _cCF