| 000 | 03785nlm1a2200529 4500 | ||
|---|---|---|---|
| 001 | 656788 | ||
| 005 | 20231030041444.0 | ||
| 035 | _a(RuTPU)RU\TPU\network\23268 | ||
| 090 | _a656788 | ||
| 100 | _a20171213a2017 k y0engy50 ba | ||
| 101 | 0 | _aeng | |
| 135 | _adrcn ---uucaa | ||
| 181 | 0 | _ai | |
| 182 | 0 | _ab | |
| 200 | 1 |
_aSol–gel synthesis and characterization of two-component systems based on MgO _fA. A. Vedyagin [et al.] |
|
| 203 |
_aText _celectronic |
||
| 300 | _aTitle screen | ||
| 320 | _a[References: p. 618 -619 (36 tit.)] | ||
| 330 | _aA series of two-component MOx–MgO systems, where M is Cu, Ni, Co, Fe, Mo or W, was synthesized by sol–gel technique. Aqueous solution of inorganic salt-precursor was used as a hydrolyzing agent. Initial xerogels and final oxides were characterized using X-ray diffraction analysis, scanning electron microscopy and low-temperature nitrogen adsorption. Decomposition of xerogels was studied by differential thermal analysis. According to X-ray diffraction analysis, all xerogel samples are characterized with turbostratic structures regardless of nature of the second component. At the same time, presence of inorganic salt in magnesium hydroxide matrix shifts the temperature of decomposition of latter towards lower values. Structural and textural characteristics of MgO-based oxide systems were found to be strongly affected by the additive. Formation of joint phase was observed in the case of cobalt oxide. In most cases, additives turned out to be even distributed in the bulk of MgO, except for WO3. This oxide formed large agglomerates because of low solubility of precursor. | ||
| 333 | _aРежим доступа: по договору с организацией-держателем ресурса | ||
| 461 | _tJournal of Sol-Gel Science and Technology | ||
| 463 |
_tVol. 82, iss. 2 _v[P. 611-619] _d2017 |
||
| 610 | 1 | _aэлектронный ресурс | |
| 610 | 1 | _aтруды учёных ТПУ | |
| 610 | 1 | _asol-gel synthesis | |
| 610 | 1 | _aMgO | |
| 610 | 1 | _atwo-component oxide systems | |
| 610 | 1 | _acharacterization | |
| 610 | 1 | _aоксид магния | |
| 610 | 1 | _aдвухкомпонентные оксидные системы | |
| 610 | 1 | _aсоли | |
| 610 | 1 | _aгели | |
| 610 | 1 | _aсинтез | |
| 610 | 1 | _aхарактеристики | |
| 701 | 1 |
_aVedyagin _bA. A. _cChemist _cChief Expert of Tomsk Polytechnic University, Candidate of chemical sciences _f1975- _gAleksey Anatolievich _2stltpush _3(RuTPU)RU\TPU\pers\36694 |
|
| 701 | 1 |
_aMishakov _bI. V. _cchemist _cAssociate Professor of Tomsk Polytechnic University, candidate of chemical sciences _f1977- _gIljya Vladimirovich _2stltpush _3(RuTPU)RU\TPU\pers\36375 |
|
| 701 | 1 |
_aKarnaukhov _bT. M. _gTimofey Mikhaylovich |
|
| 701 | 1 |
_aKrivoshapkina _bE. F. _gElena |
|
| 701 | 1 |
_aIljina _bE. V. _gEkaterina |
|
| 701 | 1 |
_aMaksimova _bT. A. _gTatjyana |
|
| 701 | 1 |
_aCherepanova _bS. V. _gSvetlana |
|
| 701 | 1 |
_aKrivoshapkin _bP. V. _gPavel |
|
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет (ТПУ) _bИнститут природных ресурсов (ИПР) _bКафедра физической и аналитической химии (ФАХ) _h94 _2stltpush _3(RuTPU)RU\TPU\col\18656 |
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет (ТПУ) _bЭнергетический институт (ЭНИН) _bКафедра атомных и тепловых электростанций (АТЭС) _h118 _2stltpush _3(RuTPU)RU\TPU\col\18683 |
| 801 | 2 |
_aRU _b63413507 _c20171213 _gRCR |
|
| 856 | 4 | _uhttps://doi.org/10.1007/s10971-017-4321-3 | |
| 942 | _cCF | ||