| 000 | 02593nlm1a2200421 4500 | ||
|---|---|---|---|
| 001 | 659665 | ||
| 005 | 20231030041637.0 | ||
| 035 | _a(RuTPU)RU\TPU\network\28352 | ||
| 035 | _aRU\TPU\network\28047 | ||
| 090 | _a659665 | ||
| 100 | _a20190314a2019 k y0engy50 ba | ||
| 101 | 0 | _aeng | |
| 135 | _adrcn ---uucaa | ||
| 181 | 0 | _ai | |
| 182 | 0 | _ab | |
| 200 | 1 |
_aFlow Synthesis of Iodonium Trifluoroacetates through Direct Oxidation of Iodoarenes by Oxone® _fN. S. Soldatova [et al.] |
|
| 203 |
_aText _celectronic |
||
| 300 | _aTitle screen | ||
| 320 | _a[References: 22 tit.] | ||
| 330 | _aFlow chemistry is considered to be a versatile and complementary methodology for the preparation of valuable organic compounds. We describe a straightforward approach for the synthesis of iodonium trifluoroacetates through the direct oxidation of iodoarenes in a simple flow reactor using an Oxone?filled cartridge. Optimization has been carried out using the Nelder–Mead algorithm. The procedure allows a wide range of iodonium salts to be prepared from simple starting materials. | ||
| 333 | _aРежим доступа: по договору с организацией-держателем ресурса | ||
| 461 | _tEuropean Journal of Organic Chemistry | ||
| 463 |
_tVol. 2019, iss. 10 _v[P. 2081-2088] _d2019 |
||
| 610 | 1 | _aэлектронный ресурс | |
| 610 | 1 | _aтруды учёных ТПУ | |
| 610 | 1 | _acontinuous flow | |
| 610 | 1 | _aoxone iodonium salts | |
| 610 | 1 | _anelder-mead method | |
| 610 | 1 | _aoxidation | |
| 610 | 1 | _aметод Нелдера–Мида | |
| 701 | 1 |
_aSoldatova _bN. S. _corganic chemist _cengineer of Tomsk Polytechnic University _f1992- _gNataliya Sergeevna _2stltpush _3(RuTPU)RU\TPU\pers\36289 |
|
| 701 | 1 |
_aPostnikov _bP. S. _corganic chemist _cSenior Lecturer of Tomsk Polytechnic University, Candidate of chemical sciences _f1984- _gPavel Sergeevich _2stltpush _3(RuTPU)RU\TPU\pers\31287 |
|
| 701 | 1 |
_aYusubov _bM. S. _cchemist _cProfessor of Tomsk Polytechnic University, Doctor of chemical sciences _f1961- _gMekhman Suleiman-Ogly (Suleimanovich) _2stltpush _3(RuTPU)RU\TPU\pers\31833 |
|
| 701 | 1 |
_aVirt _bT. |
|
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет _bИсследовательская школа химических и биомедицинских технологий (ИШХБМТ) _c(2017- ) _h8120 _2stltpush _3(RuTPU)RU\TPU\col\23537 |
| 801 | 2 |
_aRU _b63413507 _c20190314 _gRCR |
|
| 856 | 4 | _uhttps://doi.org/10.1002/ejoc.201900220 | |
| 942 | _cCF | ||