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182 0 _ab
200 1 _aThermal stability of Ti-45Nb mechanically alloyed powder
_fZh. G. Kovalevskaya [et al.]
203 _aText
_celectronic
300 _aЗаглавие с экрана
300 _aТекст на английском языке
320 _a[References: p. 447 (19 tit.)]
330 _aThe thermal stability of Ti-45Nb powder obtained via mechanical alloying of pure components Ti and Nb using an AGO-2C high energy planetary ball mill was studied. To evaluate the structure and phase transformations in the material, scanning and transmission electron microscopic studies and x-ray diffraction analysis were carried out. Mechanical alloying of titanium and niobium powders occurs under the conditions of severe plastic deformation and leads to the homogenization of initial components. As a result, an alloy with the structure consisting of a mixture of different grains is formed. This mixture of nanosized grains consists of the main ?-TiNb phase and metastable ?- and ?"-phases. The presence of metastable phases, large amount of interfaces, lattice distortions of the main phase indicate the presence of high internal energy stored in the material. By means of differential scanning calorimetric analysis it was found that structural and phase transformations occurred during heating of the powder up to temperatures of about 500°C and 700°C. During annealing at 500°C the mechanically alloyed powder loses the metastable ?"-phase while the ?-phase becomes equilibrium. At the same time, the process of recrystallization nuclei formation starts in the structure. The annealing at 700°C does not change the phase composition of the alloy. The exothermal effect observed at this temperature is related to structural transformations in the alloy, in other words, to the recrystallization of plastically deformed material. Basing on the results obtained it was concluded, that the upper limit of the thermal stability of mechanically alloyed Ti-45Nb powder does not exceed 500°C.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tПисьма о материалах
_lLetters on Materials
_fРоссийская академия наук (РАН), Институт проблем сверхпластичности металлов (ИПСМ)
_d2011-
463 _tТ. 8, № 4 (32)
_v[С. 443-447]
_d2018
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aмеханическое легирование
610 1 _aмельницы
610 1 _aпорошки
610 1 _aтермостабильность
610 1 _aотжиг
701 1 _aKovalevskaya
_bZh. G.
_cspecialist in materials science
_cAssociate Professor of Tomsk Polytechnic University, Candidate of Technical Sciences
_f1967-
_gZhanna Gennadievna
_2stltpush
_3(RuTPU)RU\TPU\pers\32481
701 1 _aSharkeev
_bYu. P.
_cphysicist
_cProfessor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences
_f1950-
_gYury Petrovich
_2stltpush
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701 1 _aKhimich
_bM. A.
_gMargarita Andreevna
701 1 _aGlukhov
_bI. A.
_gIvan Aleksandrovich
712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИнженерная школа новых производственных технологий
_bОтделение материаловедения
_h7871
_2stltpush
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712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИсследовательская школа физики высокоэнергетических процессов
_c(2017- )
_h8118
_2stltpush
_3(RuTPU)RU\TPU\col\23551
801 2 _aRU
_b63413507
_c20190513
_gRCR
856 4 _uhttps://elibrary.ru/item.asp?id=36819853
856 4 _uhttps://doi.org/10.22226/2410-3535-2018-4-443-447
942 _cCF