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100 _a20210121a2020 k y0engy50 ba
101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aModification of the microstructure and properties of martensitic steel during ultra-high dose high-intensity implantation of nitrogen ions
_fA. I. Ryabchikov, D. O. Sivin, O. S. Korneva [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: 24 tit.]
330 _aIn this work, we report a study of the chemical and phase composition, structural modifications and mechanical properties of martensitic stainless steel surface layers modified by high-intensity nitrogen ion implantation using a high current beam of low-energy nitrogen ions. The effect of ultrahigh-dose implantation of nitrogen ions into steel using a high-intensity repetitively pulsed beam of nitrogen ions with a current of 0.6 A (at an ion energy of 1.2 keV) and a sample temperature of 500 °C is investigated. The fluence of ion irradiation in the range from 6 ? 1021 ions/cm2 to 2.25 ? 1021 ions/cm2 varied by changing the current density and implantation time. The studies performed using transmission electron microscopy and X-Ray diffraction analysis of the microstructure and phase composition of the implanted samples showed that the surface-doped layer formed up to 75 ?m thick and contains ferrite, iron nitride Fe4N, and chromium nitride CrN (?-phase – 70.88 vol.%, ?'-Fe4N – 16.30 vol.%, CrN – 12.82 vol.%). The obtained values of the coherent scattering region size of the formed chromium nitride and iron nitride indicate a very high dispersion of the elements in the ion-doped layer substructure. The data on changes in the surface morphology and microhardness of the near-surface layers are presented.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tSurface and Coatings Technology
463 _tVol. 388
_v[125557, 7 p.]
_d2020
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _alow-energy nitrogen ion
610 1 _ahigh-intensity implantation
610 1 _aultra-high dose implantation
610 1 _amartensitic stainless steel
610 1 _aионы азота
610 1 _aвысокоинтенсивные технологии
610 1 _aимплантация
610 1 _aнержавеющая сталь
701 1 _aRyabchikov
_bA. I.
_cProfessor of Tomsk Polytechnic University, Doctor of physical and mathematical sciences
_cphysicist
_f1950-
_gAleksandr Ilyich
_2stltpush
_3(RuTPU)RU\TPU\pers\30912
701 1 _aSivin
_bD. O.
_cphysicist
_cSenior researcher of Tomsk Polytechnic University, Candidate of technical sciences
_f1978-
_gDenis Olegovich
_2stltpush
_3(RuTPU)RU\TPU\pers\34240
701 1 _aKorneva
_bO. S.
_cphysicist
_cengineer of Tomsk Polytechnic University
_f1988-
_gOlga Sergeevna
_2stltpush
_3(RuTPU)RU\TPU\pers\37178
701 1 _aBozhko
_bI. A.
_cphysicist
_cAssociate Professor of Tomsk Polytechnic University, Candidate of physical and mathematical sciences
_f1980-
_gIrina Aleksandrovna
_2stltpush
_3(RuTPU)RU\TPU\pers\34206
701 1 _aIvanova
_bA. I.
_cphysicist
_cAssociate Scientist of Tomsk Polytechnic University
_f1987-
_gAnna Ivanovna
_2stltpush
_3(RuTPU)RU\TPU\pers\36986
712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИнженерная школа ядерных технологий
_bНаучная лаборатория высокоинтенсивной имплантации ионов
_h7868
_2stltpush
_3(RuTPU)RU\TPU\col\23698
801 2 _aRU
_b63413507
_c20210121
_gRCR
856 4 _uhttps://doi.org/10.1016/j.surfcoat.2020.125557
942 _cCF