000 02827nlm1a2200349 4500
001 663189
005 20231030041846.0
035 _a(RuTPU)RU\TPU\network\34358
035 _aRU\TPU\network\19533
090 _a663189
100 _a20210128a2019 k y0engy50 ba
101 0 _aeng
102 _aUS
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aSynthesis of Tungsten Carbide-Filled Multiwalled Carbon Nanotubesby DC Arc Discharge Plasma in Ambient Air
_fA. Ya. Pak, Yu. Z. Vasiljeva (Vassilyeva)
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: 22 tit.]
330 _aIn this paper, the possibility of synthesizing multiwalled carbon nanotubes (CNTs) by DC arc discharge plasma in ambient air is shown. The synthesis takes place in a graphite cathode with a crucible shape using tungsten powder as a catalyst. In the non-vacuum synthesis method the CO atmosphere is generated in the reaction zone during the arcing, preventing the products of the synthesis from oxidation. According to the X-ray diffraction analysis (XRD), the synthesized product includes more than 85 vol % of carbon crystalline phases with a graphite-like structure, a cubic tungsten phase, and two phases of tungsten carbide WC and W2C. The transmission electron microscopy data shows that the product of the synthesis contains CNTs with a relatively large number of walls (up to ~50 pcs) (MWCNTs) with a diameter of up to ~100 nm and a length of up to ~1.5 µm. It was found that crystalline objects corresponding in structure to WC tungsten carbide are identified inside CNTs.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tNanotechnologies in Russia
463 _tVol. 14, iss. 11-12
_v[P. 531-535]
_d2019
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
700 1 _aPak
_bA. Ya.
_cspecialist in the field of electrical engineering
_chead of Department of Tomsk Polytechnic University, candidate of technical Sciences
_f1986-
_gAleksandr Yakovlevich
_2stltpush
_3(RuTPU)RU\TPU\pers\34120
701 1 _aVasiljeva (Vassilyeva)
_bYu. Z.
_cspecialist in the field of electric power engineering
_cResearch Engineer of Tomsk Polytechnic University
_f1995-
_gYuliya Zakharovna
_2stltpush
_3(RuTPU)RU\TPU\pers\46740
712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИнженерная школа энергетики
_bНаучно-исследовательский центр "Экоэнергетика 4.0"
_h8382
_2stltpush
_3(RuTPU)RU\TPU\col\27583
801 2 _aRU
_b63413507
_c20210128
_gRCR
856 4 _uhttps://doi.org/10.1134/S1995078019060120
942 _cCF