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101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aEffect of fast cooling on defects level, microstructure and magnetic properties of LiTiZn ferrite ceramics
_fA. V. Malyshev, A. B. Petrova, A. N. Sokolovsky, A. P. Surzhikov
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: 32 tit.]
330 _aMethod for defects level estimating by the analysis of temperature dependences of initial permeability was applied to LiTiZn ferrite ceramics. It was shown that samples of ferrite ceramics sintered in the fast cooling regime have higher defects level compare to slow cooling regime. This result confirmed by XRD. The method has a higher sensitivity compare to typical X-ray methods. The average grain sizes for both types of samples were similar. Besides they are highly agglomerated and show large grain size dispersion and also pores. Such microstructures also explain the decreased saturation magnetization for fast-cooled samples. The Cure point differs by about 20° for these sample types due to non-stoichiometry on oxygen. The obtained results can be used on industrial products of soft ferrite ceramics for defects monitoring.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tMaterials Chemistry and Physics
463 _tVol. 227
_v[P. 219-223]
_d2019
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aLiTiZn ferrites
610 1 _ainitial permeability
610 1 _acure point
610 1 _adefects level
610 1 _aферриты
610 1 _aпроницаемость
701 1 _aMalyshev
_bA. V.
_cSpecialist in the field of electrical engineering
_cSenior researcher at Tomsk Polytechnic University, Candidate of Physics and Mathematics (PhD Phys.-Math.)
_f1978-
_gAndrei Vladimirovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30965
701 1 _aPetrova
_bA. B.
_cspecialist in the field of non-destructive testing
_cAssociate Scientist of Tomsk Polytechnic University
_f1992-
_gAnna Borisovna
_2stltpush
_3(RuTPU)RU\TPU\pers\36438
701 1 _aSokolovsky
_bA. N.
_gAleksey Nikolaevich
701 1 _aSurzhikov
_bA. P.
_cphysicist
_cProfessor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc)
_f1951-
_gAnatoly Petrovich
_2stltpush
_3(RuTPU)RU\TPU\pers\30237
712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИнститут неразрушающего контроля
_bПроблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников
_h194
_2stltpush
_3(RuTPU)RU\TPU\col\19033
801 2 _aRU
_b63413507
_c20210408
_gRCR
856 4 _uhttps://doi.org/10.1016/j.matchemphys.2019.02.022
942 _cCF