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|---|---|---|---|
| 001 | 665405 | ||
| 005 | 20231030042002.0 | ||
| 035 | _a(RuTPU)RU\TPU\network\36604 | ||
| 035 | _aRU\TPU\network\28947 | ||
| 090 | _a665405 | ||
| 100 | _a20210922a2018 k y0engy50 ba | ||
| 101 | 0 | _aeng | |
| 102 | _aUS | ||
| 135 | _adrcn ---uucaa | ||
| 181 | 0 | _ai | |
| 182 | 0 | _ab | |
| 200 | 1 |
_aThe Simultaneous Voltammetric Determination of Aflatoxins В1 and М1 on a Glassy-Carbon Electrode _fG. B. Slepchenko, T. M. Gindullina, M. A. Gavrilova, A. Zh. Auelbekova |
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| 203 |
_aText _celectronic |
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| 300 | _aTitle screen | ||
| 320 | _a[References: 24 tit.] | ||
| 330 | _aFor the first time, the possibility of using stripping voltammetry for the simultaneous determination of aflatoxins C1 and N1 on a glassy-carbon electrode has been shown. +e influence of various factors (F[upsilon], [tau][upsilon], w, and the nature of the background electrolyte) on the potential and magnitude of the oxidation current of mycotoxins has been estimated. Working conditions for voltammetric determination and reproducibility of analytical signals for two mycotoxins have been selected. +e mutual influence of aflatoxins C1 and N1 on the value of analytical signals in their simultaneous presence has been studied. It has been found that, in the range of their detectable contents, the presence of aflatoxin C1 reduces the analytical signal of aflatoxin N1 by 45-50%, but the linearity of the calibration dependence is preserved. +e content of aflatoxin N1 in determination of aflatoxin B1 does not exert a significant effect in the range of 10-15%. Based on the results obtained, a procedure has been proposed for determining the content of aflatoxins C1 and N1 in their joint presence in milk by voltammetry in the concentration ranges 2•10-3-:2•101 mg/dm3 and 2•10-4-:2•102 mg/dm3 , respectively (Sr not more than 18%). | ||
| 461 | _tJournal of Analytical Methods in Chemistry | ||
| 463 |
_tVol. 2018 _v[6285623, 6 p.] _d2018 |
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| 610 | 1 | _aэлектронный ресурс | |
| 610 | 1 | _aтруды учёных ТПУ | |
| 610 | 1 | _aвольтамперометрическое определение | |
| 610 | 1 | _aафлатоксины | |
| 610 | 1 | _aстеклоуглеродные электроды | |
| 610 | 1 | _aвольтамперометрия | |
| 701 | 1 |
_aSlepchenko _bG. B. _cChemist _cProfessor of Tomsk Polytechnic University, Doctor of chemical sciences _f1956- _gGalina Borisovna _2stltpush _3(RuTPU)RU\TPU\pers\33018 |
|
| 701 | 1 |
_aGindullina _bT. M. _cChemist _cAssociate Professor of Tomsk Polytechnic University, Candidate of chemical sciences _f1951- _gTatiana Mikhailovna _2stltpush _3(RuTPU)RU\TPU\pers\33021 |
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| 701 | 1 |
_aGavrilova _bM. A. _gMariya |
|
| 701 | 1 |
_aAuelbekova _bA. Zh. |
|
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет _bИсследовательская школа химических и биомедицинских технологий _c(2017- ) _h8120 _2stltpush _3(RuTPU)RU\TPU\col\23537 |
| 712 | 0 | 2 |
_aНациональный исследовательский Томский политехнический университет _bИнженерная школа природных ресурсов _bОтделение химической инженерии _h8085 _2stltpush _3(RuTPU)RU\TPU\col\23513 |
| 801 | 2 |
_aRU _b63413507 _c20210922 _gRCR |
|
| 856 | 4 | _uhttps://doi.org/10.1155/2018/6285623 | |
| 942 | _cCF | ||