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100 _a20211215a2021 k y0engy50 ba
101 0 _aeng
135 _adrcn ---uucaa
181 0 _ai
182 0 _ab
200 1 _aCharacterization of multilayer coatings of aluminium, tungsten and molybdenum on steel substrate using laser-induced breakdown spectroscopy
_fM. Imran, Wu Ding, H. Sattar [et al.]
203 _aText
_celectronic
300 _aTitle screen
320 _a[References: 22 tit.]
330 _aLaser induced breakdown spectroscopy (LIBS) has been applied for the depth profiling of multilayer metallic coating structure which is simulated to the ITER-like wall materials in fusion devices such as EAST tokamak. The coatings were produced by magnetron sputtering and characterized by LIBS using a Nd:YAG laser at 1064 nm with pulse duration of 5 ns. The light from the resulting plasma was analyzed as a function of both number of laser pulse (N) and elemental spectral line intensity. The depth profile of the multilayer coating was determined by three different spectral signal processing methods; intensity background subtraction, intensity normalization and linear Pearson correlation. The intensity normalization method provides the best outcomes/solutions for thickness measurement and analysis of interfaces of multilayer coatings among other methods. The evolution of spectral intensity representing different materials was properly examined for 90 consecutive laser shots at the same spot. The ablation behaviour of the coating materials was analyzed in terms of ablation rate under the laser pulse of various fluences. In a much deep crater, some factors originating from laser ablation, such as material re-deposition and plasma shielding effect were analyzed. As a comparison, the depth, shape and diameter of craters were also measured using SEM and a profilometer. The influence of laser power density on the ablation rate and crater profile was investigated. The elemental composition, inside the crater, was verified by the EDX technique. The results indicate that LIBS has a potential power for in-situ depth profiling of multilayer coatings on the wall of the EAST.
333 _aРежим доступа: по договору с организацией-держателем ресурса
461 _tJournal of Nuclear Materials
463 _tVol. 544
_v[152661, 12 p.]
_d2021
610 1 _aэлектронный ресурс
610 1 _aтруды учёных ТПУ
610 1 _aLIBS stratigraphy
610 1 _aPFCs
610 1 _adepth profile of multilayer
610 1 _amagnetron sputtering
610 1 _aablation rate
610 1 _aEAST
610 1 _aмагнетронное напыление
610 1 _aабляция
610 1 _aстратиграфия
610 1 _aмногослойные покрытия
610 1 _aстальные подложки
610 1 _aспектроскопия
610 1 _aлазерный пробой
701 1 _aImran
_bM.
_gMuhammad
701 0 _aWu Ding
701 1 _aSattar
_bH.
_gHarse
701 1 _aAmir
_bM.
_gMuhammad
701 0 _aZhong-Lin He
701 1 _aHai
_bR.
_gRan
701 1 _aGupta
_bP. D.
_gPinaki Das
701 1 _aRemnev (Remnyov)
_bG. E.
_cphysicist
_cProfessor of Tomsk Polytechnic University, Doctor of technical sciences
_f1948-
_gGennady Efimovich
_2stltpush
_3(RuTPU)RU\TPU\pers\31500
701 1 _aDing
_bH.
_gHongbin
712 0 2 _aНациональный исследовательский Томский политехнический университет
_bИнженерная школа новых производственных технологий
_bНаучно-производственная лаборатория "Импульсно-пучковых, электроразрядных и плазменных технологий"
_h7882
_2stltpush
_3(RuTPU)RU\TPU\col\23502
801 2 _aRU
_b63413507
_c20211215
_gRCR
856 4 _uhttps://doi.org/10.1016/j.jnucmat.2020.152661
942 _cCF